Assoc. Prof. Dr. Daniel Kiener

Function: Group Leader
Room: 412
Phone: +43 (0) 3842-804-412
E-Mail: daniel.kiener(at)unileoben.ac.at

 

Research

Micro- and Nanomechanics and Micro- and Nanostructure Characterization

When the material grain size or the sample volume itself are reduced to the micron- and sub-micron regime, significant size effects on the mechanical properties arise due to the increased contribution of surfaces and interfaces. We aim to derive a mechanistic understanding of the interplay between sample or microstructure size, the presence of individual microstructural elements such as interfaces, grain boundaries or dislocations, and the resulting global material properties. This is achieved by a combination of sophisticated methods such as highly localized and miniaturized quantitative experiments performed within high-resolution electron microscopy techniques, temperature- and rate dependent thermo-mechanical microstructure analysis, and advanced nanoindentation techniques. Various interests in the field of Micro- and Nanomechanics concern:

  • Miniaturized testing techniques (compression, tension, bending, fracture, fatigue, ...)
  • Small scale sample preparation techniques
  • Quantitative electron microscopy
  • Size effects influencing material properties
  • Dislocation plasticity in confined volumes
  • Deformation mechanisms in nanoscale or nanostructured materials (slip, twinning, grain boundaries)
  • Irradiation resistant materials by microstructural design
  • Temperature dependent deformation mechanisms of single crystal and nanocrystalline fcc and bcc metals
  • Thermal fatigue behavior and microstructural stability of metallic thin films
  • Local depth-dependent residual stresses in complex layered structures
  • Fracture processes and properties of small structures and multilayers
  • Deformation mechanisms in hexagonal metals
  • Temperature dependent deformation mechanisms in nanoporous materials

 

Methods

Size effects influencing material properties, dislocation plasticity in confined volumes, temperature and irradiation dependent deformation, thermal fatigue and fracture of small-scale structures and multilayers, in-situ micromechanical testing in the SEM, in-situ nanomechanical testing in the TEM, advanced nanoindentation techniques, digital image correlation methods

 

  • In situ micromechanical experiments in the SEM
  • In situ nanomechanical testing in the TEM
  • Broad ion beam and FIB based material structuring
  • Advanced nanoindentation techniques (e.g. elevated temperatures, rate dependencies)
  • Digital image correlation techniques to measure local deformations and microstructural evolution
  • Local determination of residual stresses with high depth resolution
  • Miniaturized fracture testing in the SEM and TEM
  • Novel laser-based fast thermo-mechanical heating/cycling techniques

 

Teaching

In-situ an In-operando Characterization Techniques in Materials Science (In-situ und in-operando Charakterisierungstechniken in der Werkstoffwissenschaft), Materialphysik I and III, Wissenschaftliche Arbeiten in der Materialphysik

 

  • Introduction to Materials Science
  • Materials Characterization
  • Materials Physics I
  • Materials Physics III
  • Exercises to Materials Physics
  • In-situ and in-operando characterization techniques in material science
  • Exercises to In-situ and in-operando characterization techniques in material science
  • Seminar Bachelor Thesis
  • Seminar Master Thesis
  • Scientific Work in Materials Physics

Publications

  • Extraction of Flow Behavior and Hall-Petch Parameters Using a Nanoindentation Multiple Sharp Tip Approach
    A. Leitner, V. Maier-Kiener, D. Kiener
    Adv. Eng. Mater.19, UNSP 1600669 (2017)
  • Extracting flow curves from nano-sized metal layers in thin film systems
    D. Kozic, V. Maier-Kiener, R. Konetschnik, H.P. Gänser, T. Antretter, R. Brunner, D. Kiener
    Schripta Materialia130, 143-147 (2017)
  • Selective interface toughness measurements of layered thin films
    R. Konetschnik, R. Daniel, R. Brunner, D. Kiener
    AIP Advances7, ARTN 035307)
  • Strength distribution and fracture analyses of LiNbO3and LiTaO3single crystals under biaxial loading
    M. Gruber, I. Kraleva, P. Supancic, J. Bielen, D. Kiener, R. Bermejo
    Journal of the European Ceramic Society37, 4397-4406 (2017)
  • The influence of microstructure on the cyclic deformation and damage of copper and an oxide dispersion strengthened steel studied via in-situ micro-beam bending
    C. Howard, R. Fritz, M. Alfreider, D. Kiener, P. Hosemann
    Materials Science and Engineering A687, 313-322 (2017)
  • Accelerated thermo-mechanical fatigue of copper metallizations studied by pulsed laser heating
    S. Wurster, S. Bigl, M.J. Cordill, D. Kiener
    Microelectronic Engineering167, 110-118 (2017)
  • Correlative microstructure and topography informed nanoindentation of copper films
    S. Bigl, T. Schöberl, S. Wurster, M.J. Cordill, D. Kiener
    Surface & Coatings Technology, 404-413 (2016)
  • Interface dominated mechanical properties of ultra-fine grained and nanoporous Au at elevated temperatures
    A. Leitner, V. Maier-Kiener, J. Joeng, M.D. Abad, P. Hosemann, S.H. Oh, D. Kiener
    Acta Materialia121, 104-116 (2016)
  • The effect of size on the strength of FCC metals at elevated temperatures: annealed copper
    J.M. Wheeler, C. Kirchlechner, J. Micha, J. Michler, D. Kiener
    Philosophical Magazine, 3379-3395 (2016)
  • Ductilisation of tungsten (W) through cold-rolling: R-curve behaviour
    J. Reiser, S. Wurster, J. Hoffmann, S. Bonk, C. Bonnekoh, D. Kiener, R. Pippan, A. Hoffmann, M. Rieth
    Int. J. Refract. Met. Hard Mat.58, 22-33 (2016)